Search results for "Diffusion des rayons X"
showing 1 items of 1 documents
Préparation et spéciation d’oxo-clusters de métaux du bloc p
2022
The main subject of this thesis is the use of Pair Distribution Function (PDF) analysis for solution phase speciation during metal-cluster growth. The PDF method allows the extraction of structural information from a sample in the form of an atom-atom distance distribution via Fourier transform of synchrotron X-ray scattering data. The growth mechanisms of two solution-based systems are analysed in this thesis. Precursor materials are synthesized through a mechanochemical method that was developed and shown to be able to access a wide range of related systems.Mechanochemical routes of synthesizing bismuth Active Pharmaceutical Ingredients (APIs) were investigated and optimised. Samples were…